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LC-HRMS measurements have been in accordance Together with the structures advised from NMR measurements and isotopic designs confirmed the existence with the three halogen atoms claimed with the provider.
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As revealed before, chiral HPLC columns according to derivatized polysaccharides for example amylose or cellulose are well suited for chiral separation of the wide spectrum of NPS [18,19,20]. According to these findings, a Lux i-Amylose-one column was decided on for your chiral separation experiments on the a few four-methylaminorex derivatives. Success of chiral HPLC combined with NMR-findings exposed that all three analytes were being present as racemic mixtures from the trans diastereomer.
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